Engenharia de Materiais
URI permanente desta comunidadehttps://repositorio.fei.edu.br/handle/FEI/17
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6 resultados
Resultados da Pesquisa
- Nanocomposites of PLA/ZnO nanofibers for medical applications: Antimicrobial effect, thermal, and mechanical behavior under cyclic stress(2022-01-18) NONATO, R.C.; MEI, L.H.I.; Baltus Cornelius Bonse; LEAL, C.V.; LEVY, C.E.; OLIVEIRA, F.A.; DELARMELINA, C.; DUARTE, M.C.T.; MORALES, A.R.The application of biodegradable and biocompatible polymer poly(lactic acid) (PLA) in the medical field has been widely studied. In this study, films of neat PLA and PLA containing 1 wt% ZnO nanofibers obtained by electrospinning (PLA/ZnO) were successfully molded by solvent-cast three-dimensional (3D) printing. Mechanical behavior was assessed by conventional dynamic mechanical analysis (DMA) and by adapting the equipment conditions to simulate a mechanical fatigue test at human body temperature—cyclic stress in isotherm at 36.5°C. DMA results showed that for temperatures above 30°C, the storage module of PLA/ZnO was higher when compared to neat PLA, and in the fatigue test, PLA/ZnO withstood more than 3600 cycles while neat PLA failed after an average of 1768 cycles. Differential scanning calorimetry (DSC) tests revealed that cyclic stress did not cause changes in the degree of crystallinity of the PLA. The microdilution and plating methods were applied to bacteria (Staphylococcus aureus, Salmonella, and Escherichia coli) and to yeast (Candida albicans) and revealed the antimicrobial effect of ZnO nanofibers and the PLA/ZnO composite. The antimicrobial activity and fatigue resistance of PLA/ZnO nanocomposites indicate that the material has potential for application in bone implants.
- Reduced order modeling of composite laminates through solid-shell coupling(2017) Salerno G.; Mariani S.; Corigliano A.© 2017, Journal of Aerospace Technology and Management. All rights reserved.Composite laminates display a complex mechanical behavior due to their microstructure, with a through-thickness variation of the displacement and stress fields that depends on the fiber orientation in each layer. Aiming to develop reduced-order numerical models mimicking the real response of composite structures, we investigated the capability and accuracy of finite element analyses coupling layered shell and solid kinematics. This study represents the first step of a work with the goal of accurately matching stress evolution in regions close to possible impact locations, where delamination is expected to take place, with reduced computational costs. Close to such locations, a 3-D modeling is adopted, whereas in the remainder of the structure, a less computationally demanding shell modeling is chosen. To test the coupled approach, results of numerical simulations are presented for a quasi-statically loaded cross-ply orthotropic plate, either simply supported or fully clamped along its boundary.
- Effect of Mo substitution by W on the passive characteristics and mechanical properties of AISI 316L austenitic stainless steel(2019) Terra B.C.M.; Magnabosco R.© 2019 NACE International.This work studied the influence on pitting corrosion resistance and mechanical behavior of the partial or total substitution of Mo by W in AISI 316L austenitic stainless steel. Alloys that contain 0%, 25%, 50%, 75%, or 100% of Mo substitution by W in atomic content were produced and analyzed. Microstructural analysis showed that W does not cause any difference in the size, distribution, and composition of inclusions. However, the grain sizes are slightly reduced in samples with W. Tensile tests did not show any difference in their mechanical properties. Cyclic polarization results do not show any difference between the samples with and without W in 3.5% NaCl at room temperature. However, the sample with 50% W and 50% Mo showed the highest critical pitting temperature in 1 M NaCl solution after potentiostatic polarization at 180 mVAg/AgCl, 40±4°C. This result shows a synergic effect of Mo and W for pitting corrosion resistance of austenitic stainless steel.
- Investigation on the effect of a compatibilizer on the fatigue behavior of PP/coir fiber composites(2011) Bettini S.H.P.; Antunes M.C.; Magnabosco R.The mechanical behavior of polypropylene (PP) and 30 wt% coir fiber reinforced PP composites, with and without compatibilizer, were assessed through monotonic (tensile and bending) and cyclic (fatigue) tests. Fatigue load controlled tests were conducted under tension loads at a frequency of 6 Hz. The fracture mechanism was accompanied by surface fracture analyses using both optical microscopy and scanning electron microscopy. The compatibilizer used was the PP grafted with maleic anhydride. The compatibilized composites exhibited longer fatigue life times. It was also concluded that the presence of coir fibers changed the preferential fatigue mechanism, because the fracture mechanism in PP was mainly caused by heat generated by viscous effects during solicitation (thermal fatigue), whereas in the compatibilized and noncompatibilized PP/coir composites the predominant fracture mechanism was mechanical fatigue. However, thermal fatigue was also observed in the composites, especially in the noncompatibilized ones. © POLYM. ENG. SCI., 2011. Copyright © 2011 Society of Plastics Engineers.
- Effect of sawdust surface treatment and compatibilizer addition on mechanical behavior, morphology, and moisture uptake of polypropylene/sawdust composites(2010) Bettini S.H.P.; Bonse B.C.; Melo E.A.; Munoz P.A.R.Polypropylene/sawdust composites were investigated to assess the effect of sawdust surface treatment and compatibilizer addition on polymer/fiber adhesion. Two silane coupling agents were used for sawdust surface treatment: vinyl-tris (2-methoxyethoxy) silane and (3- aminopropyl)triethoxysilane. Maleic anhydride grafted polypropylene was used as compatibilizer. Composites were prepared in a corotating twin-screw extruder coupled to a Haake torque rheometer and submitted to tensile and bending tests as well as scanning electron microscopy (SEM). Moisture uptake tests were also performed. Results showed that incorporation of untreated sawdust to polypropylene (PP) caused reduction in composite tensile strength and increase in stiffness. When the only treatment used was surface modification with silane coupling agents, no significant changes were observed in mechanical properties. However, when compatibilizer was added to the composites, tensile strength was increased, and % elongation at break reduced, indicating improved system compatibility. The composite presenting the highest increase in tensile strength was that containing sawdust treated with amino silane in addition to the compatibilizer. SEM analyses corroborated the mechanical property results. © 2009 Society of Plastics Engineers.
- Fatigue life of coir fiber reinforced PP composites: Effect of compatibilizer and coir fiber contents(2013) Antunes M.C.; Moraes D.V.O.; Magnabosco R.; Bonse B.C.; Bettini S.H.P.The fatigue behavior of polypropylene/coir fiber composites was investigated. Composites were prepared according to an experimental statistical design, in which the independent variables coir fiber and compatibilizer content were varied. The compatibilizer used was maleic anhydride grafted polypropylene (PP-g-MA). Compatibilizer free composites were also prepared. Composites were prepared in a corotating twin-screw extruder and the mechanical behavior of polypropylene/coir fiber composites were assessed through monotonic (tensile) and cyclic (fatigue) tests. Fatigue load controlled tests were conducted under tension-tension loads at a frequency of 6 Hz. The fracture mechanism was accompanied by surface fracture analyses using scanning electron microscopy (SEM). The results indicated the need for using compatibilizer in the composites; however, increase in compatibilizer content did not affect composite fatigue lifetime. Coir content was the variable with the strongest effect on composite properties; increasing this variable caused significant increase in fatigue life. © 2013 Society of Plastics Engineers.