Engenharia de Materiais
URI permanente desta comunidadehttps://repositorio.fei.edu.br/handle/FEI/17
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3 resultados
Resultados da Pesquisa
Artigo de evento 0 Citação(ões) na Scopus Ferrite-to-austenite transformation during cold working of a duplex stainless steel(2011-09-23) Rodrigo Magnabosco; TAVARES, D. B.; FORGAS, A.; DE MOURA NETO, C.Ferrite-austenite duplex stainless steels (DSS) are replacing austenitic stainless steels in many applications due to its high mechanical and corrosion resistance. However, magnetic measurements of ferrite volume fraction using a ferritscope of cold worked samples indicate a reduction in the ferrite content with increasing mechanical work. Considering this fact, this work studies the influence of the cold working on the ferrite/austenite ratio. Samples of UNS S31803 DSS sheet, originally 3 mm thick, were solution-treated at 1175°C for 30 minutes and water quenched; after that, different levels of cold working were applied. Ferrite volume fraction was determined using two distinct methods: quantitative stereology with an optical microscope and magnetic measurements using a ferritscope; a detailed microstructural characterization, including X-ray diffractometry, was conducted to base the discussion of a possible ferrite-to-austenite diffusionless transformation.Artigo de evento 3 Citação(ões) na Scopus Comparative study of ferrite quantification methods applied to duplex stainless steels(2011-09-23) Rodrigo Magnabosco; SPOMBERG, S.Duplex stainless steels (DSS) present approximately the same quantities of ferrite (magnetic phase) and austenite. These steels are replacing austenitic stainless steels in some applications due to its high mechanical and corrosion resistance. However, changes in the volumetric percentage of those phases can modify material properties, justifying the development of this study, which has as principal aim a comparison between three different ferrite quantification methods. Samples of two different DSS (UNS S31803 or UNS S32750), originally supplied as 20mm round bars, were solution-treated between 1000°C and 1250°C, in order to obtain different ferrite/austenite ratios. Ferrite quantification was performed in three sections: longitudinal, transverse and diagonally oriented to the rolling direction. The volume fraction of ferrite was determined using three distinct methods: quantitative stereology with an optical microscope, magnetic measurements using a ferritscope, and X-ray analysis by comparison of the relative intensities of peaks corresponding to the planes that generate maximum intensity of diffraction for single-phase samples. Results are discussed, analysing the reliability of the studied methods.- Intermetallic phases formation during short aging between 850 °c and 950 °c of a superduplex stainless steel(2012) Magnabosco R.; Dos Santos D.C.This paper is based on the study of intermetallic phase formation during aging between 850 C and 950 C, for periods up to 5 min; those treatments were conducted in liquid aluminum bath, allowing fast heating of the small sized specimens. It was found that backscattered electron images could be used in the automatized routines of quantitative stereology of intermetallic phases and nitrides found in duplex and superduplex stainless steels. A measurable intermetallic phase fraction was observed just after 1 min aging in the studied temperatures, but it was not possible to distinguish sigma and chi phases from the observed intermetallic phases. Nitrides were also observed, but they were probably formed in steel manufacturing, since there was no significant influence of aging on its volume fraction. © 2012 Elsevier Editora Ltda. and Brazilian Metallurgical, Materials and Mining Association.